Compendium of Organic Synthetic Methods Volume 6 by Michael B. Smith

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By Michael B. Smith

Presents artificial chemists with a style for fast retrieval of knowledge from the literature, directory fabric via response sort instead of via writer identify or ebook date. every one up-to-date quantity provides the newest man made tools for coaching of monofunctional and difunctional compounds. The association is logical and simple to keep on with; sections are prepared in accordance with the potential interconversions among the foremost practical teams. allows man made chemists to maintain abreast of contemporary advancements and retrieve a selected piece of data quick and simply.

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H. V. ; DeLuca, O . D . *; Nakano, Ogawa, M. *; Youngdahl, K. Y. 8H20/H20 iPrOH , ref1 ux * Matsushita, H. ; Mizusaki, S. : -Chem Lett, (1985), 731 *Jy 1 . P h 2 S b H , THF, A 1 C 1 3 RT 2. a q . ; Chen, C. Tetrahedron E, (19851, nBu3SnH, MeOH, 96% 26, 5171 55OC 1400 m P a , 24h * A. : Rahm, N. -J Org Chem, (19861, quant 51, 1672 +'" 41 ALCOHOLS F R O M KETONES SECTION 42B 1 . HSCH2CH2SH, H t 32 . R. M. SECTION 42B: Alkylation of Ketones, Forming Alcohols Aldol reactions are listed in Section 330 (Ketone-Alcohol).

8H20/H20 iPrOH , ref1 ux * Matsushita, H. ; Mizusaki, S. : -Chem Lett, (1985), 731 *Jy 1 . P h 2 S b H , THF, A 1 C 1 3 RT 2. a q . ; Chen, C. Tetrahedron E, (19851, nBu3SnH, MeOH, 96% 26, 5171 55OC 1400 m P a , 24h * A. : Rahm, N. -J Org Chem, (19861, quant 51, 1672 +'" 41 ALCOHOLS F R O M KETONES SECTION 42B 1 . HSCH2CH2SH, H t 32 . R. M. SECTION 42B: Alkylation of Ketones, Forming Alcohols Aldol reactions are listed in Section 330 (Ketone-Alcohol). 1 . PhCH2SiMe3, T H F nBu4NF, O°C PhCCH3 OH I t 2 .

Nickel boride 1 . BrCH2CH2-CH-CH Li 2. 90 (89% ee) 25, 3947 96%(69:31) 9, 869 75% (1OO:O) Fekih, A . ; Lusinchi, X. Tetrahedron L e t t , (19851, Li I 3,987 x * Zn/CH C1 / M e 2 S i C 1 -2 . S. ; Behrooz, M. -J Org Chem, ( 1 9851, 84% 2,3674 32 COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 6 1 . A. 2 . a q . A. them, (19861, -J Org 1 . : Schroeder, J . E . : Wetzel, J . M . -J Org Chem, (1 986) , 51, 4731 CH2=CHCH2SiMe3 Oku, 51, 3391 * 2 . a q . NH4V1 Hwu, J . R . OH I CH3(CH2)3CHCH3 * / \ SECTION 39 *.

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